3D打印用尼龙粉末的制备技术研究进展

艾吉祥, 邓容, 任露露, 杨敬葵

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中国高校科技期刊信息汇聚平台
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塑料科技 ›› 2024, Vol. 52 ›› Issue (04) : 148-152. DOI: 10.15925/j.cnki.issn1005-3360.2024.04.029
综述

3D打印用尼龙粉末的制备技术研究进展

作者信息 +

Research Progress on Preparation Technology of Nylon Powder 3D Printing

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History +

摘要

文章围绕3D打印用尼龙（PA）粉末的制备技术展开论述，主要介绍PA粉末三种3D打印技术方法，并对比各自特点，得出选择性激光烧结（SLS）最适合用于PA粉末3D打印。文章论述了PA粉末的制备方法，主要包括直接聚合法、机械粉碎法、溶剂沉淀法、热致相分离法，对比四种制备方法的优缺点，概述了PA粉末的改性研究，分析了影响PA粉末SLS制品的因素。研究可为从事PA粉末3D打印相关的人员提供借鉴和参考。

Abstract

This paper focuses on the preparation technology of nylon (PA) powder for 3D printing, mainly introduces three 3D printing technologies of PA powder, compares their respective characteristics, and concludes that selective laser sintering (SLS) is most suitable for 3D printing of PA powder. The preparation methods of PA powder are discussed, including direct polymerization, mechanical crushing, solvent precipitation, and thermally induced phase separation. The advantages and disadvantages of the four preparation methods are compared, the modification research of PA powder is summarized, and the factors affecting PA powder SLS products are analyzed. The research can provide a reference for people engaged in PA powder 3D printing.

关键词

尼龙粉末 / 选择性激光烧结 / 粉末制备 / 掺杂改性

Key words

Nylon powder / Selective laser sintering / Powder preparation / Doping modification

中图分类号

TQ320.66

引用本文

EndNote

Ris (Procite)

Bibtex

导出引用
艾吉祥 , 邓容 , 任露露 , 等. 3D打印用尼龙粉末的制备技术研究进展. 塑料科技. 2024, 52(04): 148-152 https://doi.org/10.15925/j.cnki.issn1005-3360.2024.04.029
AI Ji-xiang, DENG Rong, REN Lu-lu, et al. Research Progress on Preparation Technology of Nylon Powder 3D Printing[J]. Plastics Science and Technology. 2024, 52(04): 148-152 https://doi.org/10.15925/j.cnki.issn1005-3360.2024.04.029

参考文献

列表( 原文顺序 | 文献年度倒序 | 文中引用次数倒序 ) 可视化分析
1
MARTIN J, YAHATA B, HUNDLEY J, et al. 3D printing of high-strength aluminium alloys[J]. Nature, 2017, 549: 365-369.
本文引用 [1]
2
张馨月,曲成平,崔维久,等.基于数值模拟的混凝土3D打印性能分析方法研究[J].施工技术(中英文),2023,52(17):38-43.
本文引用 [1]
3
连芩,武向权,田小永,等.陶瓷增材制造[J].现代技术陶瓷,2017,38(4):267-277.
本文引用 [1]
4
LI J P, ALCOUFFEL P, MELIS F, et al. Efficient hydrosilylation reaction in polymer blending: An original approach to structure PA12/PDMS blends at multiscales[J]. Polymer, 2017, 112: 10-25.
本文引用 [1]
5
GU D, MEINERS W, WISSENBACH K, et a1. Laser additive manufacturing of metallic components:Materials,processes and mechanisms[J]. International Materials Reviews, 2013, 57(3): 133-164.
本文引用 [1]
6
SEN G S, MANOJ S V, KRISHNAN S, et al. Thermal conductivity enhancement of nano fluids containing graphene nanosheets[J]. Journal of Applied Physics, 2011, DOI: 10.1063/1.3650456.
本文引用 [1]
7
IM H, KIM J. Thermal conductivity of a graphene oxide-carbon nanotube hybrid/epoxy composite[J]. Carbon, 2012, 50(15): 5429-5440.
本文引用 [1]
8
GOODRIDGE R D, SHOFNER M L, HAGUE R, et al. Processing of a polyamide-12/carbon nanofibre composite by laser sintering[J]. Polymer Testing, 2011, 30(1): 94-100.
本文引用 [1]
9
王欣华.聚酰胺12微粉的制备及性能研究[D].北京:北京理工大学,2017.
本文引用 [1]
10
袁宗伟,王旭华.溶剂法制备粒径分布集中的PA12球形微粉[J].工程塑料应用,2018,46(6):75-78.
本文引用 [1]
11
刘宁.常压溶剂法制备聚合物粉末的工艺研究[D].北京:中国石油大学(北京),2011.
本文引用 [1]
12
朱建民.聚酰胺树脂及其应用[M].北京:化学工业出版社,2011.
本文引用 [1]
13
GUO Z, YANG Y, XIANG S,et al. Preparation of PVDF membrane based on "In-situ Template-TIPS" technology and the investigation on membrane formation mechanism, microstructure regulation and permeability[J]. Journal of Membrane Science, 2020, DOI: 10.1016/j.memsci.2020.118839.
本文引用 [1]
14
陈丽卿,吴波震,祝郑冬,等.粒径可控3D打印用PA6/12粉末制备及热性能研究[J].化工新型材料,2017,45(5):226-228.
本文引用 [1]
15
周依莎,邓鑫,焦晓岚,等.阴离子聚合PA6/木粉复合材料的制备及性能[J].塑料,2022,51(1):1-4, 47.
本文引用 [1]
16
张利建,伍千新,陶馥洁,等.原位聚合无卤阻燃3D打印PA6粉末的制备及表征[J].合成纤维工业,2018,41(1):39-42.
本文引用 [1]
17
GOODRIDGE R D, TUCK C J, HAGUG R. Laser sintering of polyamides and other polymers[J]. Progress in Materials Science, 2012, 57(2): 229-267.
本文引用 [1]
18
汤教佳,葸舒婷,张佩瑶,等.深冷粉碎制备尼龙粉末流动性的改善及选择性激光烧结性能[J].塑料工业,2018,46(7):26-31.
本文引用 [1]
19
唐城城,俞海燕,乔梁,等.选择性激光烧结用Al2O3/PA12复合材料的制备和成型[J].塑料工业,2015,42(2):130-135.
本文引用 [1]
20
金叶,高唯,孙茂银,等.选择性激光烧结用尼龙1212粉末的制备[J].工程塑料应用,2023,51(2):23-28.
本文引用 [1]
21
方亮,汪艳,陈震.3D打印用PA6∕PA12复合粉末的制备与性能[J].工程塑料应用,2019,47(2):20-24, 51.
本文引用 [1]
22
WANG G, WANG P, ZHEN Z, et al. Preparation of PA12 microspheres with tunable morphology and size for use in SLS processing[J]. Materials & Design, 2015, 87: 656-662.
本文引用 [1]
23
GUO Z, YANG Y, XIANG S, et al. Preparation of PVDF membrane based on "in-situ template-TIPS" technology and the investigation on membrane formation mechanism, microstructure regulation and permeability[J]. Journal of Membrane Science, 2020, DOI: 10.1016/j.memsci.2020.118839.
本文引用 [1]
24
SU D, YANG J K, LIU S, et al. Preparation of polyamide 12 powder for additive manufacturing applications via thermally induced phase separation[J]. e-Polymers, 2022, 22(1): 553-565.
本文引用 [1]
25
PEI A H, LIU A D, XIE T X, et al. A new strategy for the preparation of polyamide-6 microspheres with designed morphology[J]. Macromolecules, 2006, 39(23): 7801-7804.
本文引用 [1]
26
陈献,葸淑婷,黄亚江,等.聚合诱导相分离制备用于SLS的聚酰胺6球形粉末[J].塑料工业,2020,48(8):21-25, 65.
本文引用 [1]
27
WANG G X, LIU P, ZHANG Wet al. Preparation and characterization of novel PA6/SiO2 composite microsphere applied for selective laser sintering[J]. Express Polymer Letters, 2018, 12(1): 13-23.
本文引用 [1]
28
SHI Y S, YANG J S, YAN C Z, et al. An organically modified montmorillonite/nylon‐12 composite powder for selective laser sintering[J]. Rapid Prototyping Journal, 2011, 17(1): 28-36.
本文引用 [1]
29
吴婷,吴宏,文杰斌.选择性激光烧结 GB/GF/PA1212的力学与摩擦学性能[J].粉末冶金材料科学与工程,2022,27(6):569-578.
本文引用 [1]
30
张正义,陈英红,戚方伟,等.固相剪切碾磨制备尼龙12/多壁碳纳米管复合粉体及选择性激光烧结3D打印[J].高分子材料科学与工程,2017,33(3):122-127.
本文引用 [1]
31
SALMORIA G V, PAGGI R A, LAGO A,et al. Microstructural and mechanical characterization of PA12/MWCNTs nanocomposite manufactured by selective laser sintering[J]. Polymer Testing, 2011, 30(6): 611-615.
本文引用 [1]
32
黄自华,陈潜,杨旖莎,等.鳞片石墨填充PA66导热复合材料的性能.塑料,2018,47(1):9-12.
本文引用 [1]
33
于翔,赵珂,王延伟,等,张雅琪.3D打印用尼龙66/Cu复合粉体的制备与性能[J]. 高分子材料科学与工程,2018,34(9):165-170.
本文引用 [2]
34
杨秀琴,刘意鹤,苗世成,等.用于选择性激光烧结成型的聚酰胺6/硫酸钙复合粉体的制备及性能研究[J]. 中国塑料,2021,35(10):31-36.
本文引用 [1]
35
YAN C, SHI Y, YANG J, et al. Preparation and selective laser sintering of nylon-12 coated metal powders and post processing[J]. Journal of Materials Processing Tech, 2009, 209(17): 5785-5792.
本文引用 [1]
36
DRUMMER D, WUDY K, KUHNLEIN F, et al. Polymer blends for selective laser sintering: Material and process requirements[J].Physics Procedia, 2012, 39: 509-517.
本文引用 [1]
37
肖浩,周良霄,李杰,等.PEHD-g-MAH共混改性PA612性能研究[J].工程塑料应用,2020,1(48):41-45.
本文引用 [1]
38
任蕊,曹晨茜.基于高分子材料3D打印成型技术的研究[J].应用化工,2020,49(9):2370-2376.
本文引用 [1]
39
GOODRIDGE R D, DALGARNO K, WOOD D J. Indirect selective laser sintering of an apatite-mullite glass-ceramic for potential use in bone replacement applications[J].Proceedings of the Institution of Mechanical Engineers. Part H, Journal of engineering in medicine, 2006, 220(1): 57-68.
本文引用 [1]
40
SCHMID M, AMADO A, WEGENER K. Materials perspective of polymers for addiyive manufacturing with selective laser sintering[J]. Journal of Materials Research, 2014, 29(17): 1824-1832.
本文引用 [1]
41
BERRETTA S, GHITA O, EVANS K E. Morphology of polymeric powders in laser sintering (LS): From polyamide to new PEEK powers[J]. European Polymer Journal, 2014, 59: 218-229.
本文引用 [1]
42
高唯,金叶,孙茂银,等.窄粒径分布近球形PA12粉末制备及其SLS制件性能研究[J].塑料工业,2023,51(4):158-164.
本文引用 [1]
43
迟长龙,安彦飞,严亚如.溶剂与添加剂对溶剂沉淀法制备PA12 粉体的影响[J].中国塑料,2020,34(12):65-69.
本文引用 [1]
44
于翔,赵俊杰,张朋飞,等.3D打印用TiO2/PA6复合粉体的制备与性能分析[J].塑料,2017,46(3):9-13.
本文引用 [1]
45
曹毅,张雅琪,孙梦迪,等.PA1012/n-HAP复合粉体的制备及热性能和流动性表征[J].塑料科技,2018,46(1):21-25.
本文引用 [1]
46
LING Z C, WU J Z, WANG X, et al. Experimental study on the variance of mechanical properties of polyamide 6 during multi-layer sintering process in selective laser sintering[J]. The International Journal of Advanced Manufacturing Technology, 2019, 101: 1227-1234.
本文引用 [1]
47
师平,白亚琼.选择性激光烧结成型尼龙6的拉伸性能研究[J].现代塑料加工应用,2021,33(4):29-33.
本文引用 [1]
48
CAULFIELD B, MCHUGH P E, LOHFELD S. Dependence of mechanical properties of polyamide components on build parameters in the SLS process[J]. Journal of Materials Processing Technology, 2007, 182(1/3): 477-488.
本文引用 [1]
49
SINGH S, SHARMA V S, SACHDEVA A. Application of response surface methodology to analyze the effect of selective laser sintering parameters on dimensional accuracy[J].Progress in Additive Manufacturing, 2018, 4: 3-12.
本文引用 [1]
50
CZELUSNIAK T, AMORIM F L. Influence of energy density on selective laser sintering of carbon fiber-reinforced PA12[J]. International Journal of Advanced Manufacturing Technology, 2020, 111(7/8): 1-16.
本文引用 [1]

基金

贵州省省级科技计划项目 贵州省基础研究（自然科学）项目(黔科合基础-ZK［2022］一般219)
贵州省科技支撑项目(黔科合支撑［2023］一般350)
贵州省科技支撑项目(黔科合支撑［2022］一般057)

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