
Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
Qinsheng HE, Jianqiao WANG, Zhen ZHAO, Fang LI, Shiqing ZHANG, Hong WANG, Xingzheng ZOU, Yuanshou TANG, Min HUANG, Jing LI
Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire
The elastic limit is a critical parameter in spring design, which has a significant impact on the spring characteristic. The influence of cold drawing on the strength, elastic limit, elastic after-effect, and microstructure of 07Cr17Ni7Al ultrafine wire with a diameter of 0.3 mm for valve springs is investigated using room temperature tensile tests, single arm bending method, optical microscope(OM), X-ray diffraction(XRD) and scanning electron microscope(SEM). Different mathematical models are used to fit and analyze the deformation and martensite content, deformation-elastic limit, and stress-elastic after-effect. The results show that the solid solution 07Cr17Ni7Al wire is composed of austenite and a small amount of ferrite. Cold drawing transforms austenite into martensite, the content of deformation-induced martensite (DIM) increases with increasing deformation. The relationship between DIM content and cold-drawn equivalent strain (η) conforms to the Olson-Cohen model. When η reaches 1.64, the DIM content is about 92%, and the DIM reaches saturation. The tensile strength of wire exhibits a linear relationship with η, and the larger the deformation, the higher the tensile strength. The relationship between the elastic limit and the η follows an “S” shaped curve and conforms to the DoseResp model. The elastic limit increases with increasing deformation. When the η reaches 1.64 or more, the elastic limit tends to be gentle. The elastic after-effect increases with increasing stress, which conforms to the PWL2 model. There exists a “critical stress for elastic after-effect”. When the stress exceeds this critical value, the rate of elastic after-effect increases by 2-11 times with increasing stress. When the η is 1.64-2.41, the 07Cr17Ni7Al wire has good mechanical and elastic properties.
stainless steel / deformation-induced martensite / elastic limit / elastic after-effect / mechanical property / ultrafine wire / cold drawing
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