国产Al2O3f/Al2O3复合材料的室温和1000 ℃拉伸性能

张珂, 许平, 张超, 李陈晨, 应雯清, 邢宁, 李玫, 张程煜

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材料工程 ›› 2025, Vol. 53 ›› Issue (1) : 195-201. DOI: 10.11868/j.issn.1001-4381.2024.000420
研究论文

国产Al2O3f/Al2O3复合材料的室温和1000 ℃拉伸性能

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Tensile properties of domestic Al2O3f/Al2O3 composite at room temperature and 1000 ℃

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摘要

连续氧化铝纤维增强氧化铝复合材料(Al2O3f/Al2O3)是发展高性能航空发动机热端部件的理想材料。本工作研究了国产Al2O3f/Al2O3复合材料的室温和1000 ℃拉伸力学性能,使用SEM观察拉伸试样的微观形貌和断口形貌,使用TEM观察纤维的微观结构,采用Weibull分布统计分析抗拉强度,利用纤维推入法得到纤维/基体界面剪切强度。结果表明,国产Al2O3f/Al2O3复合材料室温抗拉强度为(257±31) MPa,1000 ℃的抗拉强度为室温的78%,已达到国际Nextel610/Al2O3水平。研究发现,界面结合强度是影响抗拉强度的主要因素。界面结合强度较低,纤维拔出长且分散,抗拉强度高;界面结合强度较高,发生纤维束断裂,且纤维拔出变短,抗拉强度低。

Abstract

Continuous alumina fiber reinforced alumina composite (Al2O3f/Al2O3) is an ideal material for developing high-performance aero-engine hot section components. In this study, the room-temperature and 1000 ℃ tensile mechanical properties of domestic Al2O3f/Al2O3 are investigated. The microscopic morphology and fracture morphology of tensile specimens are observed by SEM. The microstructure is observed by TEM. The tensile strength is analyzed using the Weibull distribution, and the fiber/matrix interfacial shear strength is obtained by the fiber push-in method. The results show that the room-temperature tensile strength of domestic Al2O3f/Al2O3 is (257±31) MPa while the tensile strength at 1000 ℃ is 78% of room temperature strength, reaching the level of foreign Nextel610/Al2O3. The interfacial bonding is the main factor affecting the tensile strength. High tensile strength with low interfacial bonding strength, results in long and dispersed fiber pull-out. Low tensile strength with high interfacial bonding strength, results in fiber bundle breakage and shorter fiber pull-out.

关键词

氧化铝纤维 / Al2O3f/Al2O3复合材料 / 拉伸性能 / 强度分散性 / 界面结合强度

Key words

alumina fiber / Al2O3f/Al2O3 composite / tensile property / strength dispersion / interfacial bonding strength

中图分类号

TB33 / V257

引用本文

导出引用
张珂 , 许平 , 张超 , . 国产Al2O3f/Al2O3复合材料的室温和1000 ℃拉伸性能. 材料工程. 2025, 53(1): 195-201 https://doi.org/10.11868/j.issn.1001-4381.2024.000420
Ke ZHANG, Ping XU, Chao ZHANG, et al. Tensile properties of domestic Al2O3f/Al2O3 composite at room temperature and 1000 ℃[J]. Journal of Materials Engineering. 2025, 53(1): 195-201 https://doi.org/10.11868/j.issn.1001-4381.2024.000420

参考文献

[1]
RAMACHANDRAN K LEELAVINODHAN S ANTAO C,et al.Analysis of failure mechanisms of oxide-oxide ceramic matrix composites[J].Journal of the European Ceramic Society202242(4):1626-1634.
[2]
SZWEDA A BUTNER S RUFFONI J,et al.Development and evaluation of hybrid oxide/oxide ceramic matrix composite combustor liners[C]∥ASME Turbo Expo 2005: Power for Land,Sea,and Air.Reno:ASME,2005.
[3]
BERGER M H BUNSELL A R.Oxide fibers[M].Comprehensive Composite Materials Ⅱ.Amsterdam:Elsevier,2018.
[4]
ZOK F W LEVI C G.Mechanical properties of porous matrix ceramic composites[J].Advanced Engineering Materials20013(1/2):15-23.
[5]
SIMON R A.Progress in processing and performance of porous-matrix oxide/oxide composites[J].International Journal of Applied Ceramic Technology20052(2):141-149.
[6]
JURF R A BUTNER S C.Advances in oxide-oxide CMC[J].Journal of Engineering for Gas Turbines and Power2000122(2):202-205.
[7]
杨瑞,陈易诚,邓杨芳,等.高温热暴露对Al2O3/Al2O3陶瓷基复合材料性能影响[J].航空材料学报202343(2):1-8.
YANG R.CHEN Y C.DENG Y F.Effect of high temperature thermal exposure on properties of Al2O3/Al2O3 ceramic matrix composites.[J].Journal of Aeronautical Materials202343(2):1-8.
[8]
刘海韬,姜如,孙逊,等.连续氧化铝纤维增韧陶瓷基复合材料[M].北京:科学出版社,2022:212-214.
LIU H T JIANG R SUN X,et al.Continuous alumina fiber reinforced ceramic matrix composites[M].Beijing:Science Press,2022:212-214.
[9]
YAN J JIANG D WANG X,et al.High temperature tensile property of domestic 550-grade continuous alumina ceramic fiber[J].Journal of Inorganic Materials202237(6):629.
[10]
SCHMVCKER M FLUCHT F MECHNICH P.Degradation of oxide fibers by thermal overload and environmental effects[J].Materials Science amd Engineering: A2012557(2):10-16.
[11]
DÉBARRE A JULIAN-JANKOWIAK A PARLIER M,et al.Effect of temperature on the mechanical behaviour of an oxide/oxide composite[J].Journal of the European Ceramic Society202242(15):7149-7156.
[12]
LEVI C G YANG J Y DALGLEISH B J,et al.Processing and performance of an all-oxide ceramic composite[J].Journal of the American Ceramic Society199881(8):2077-2086.
[13]
ZAWADA L P HAY R S LEE S S,et al.Characterization and high temperature mechanical behavior of an oxide/oxide composite[J].Journal of the American Ceramic Society200386(6):981-990.
[14]
RUGGLES-WRENN M B BRAUN J C.Effects of steam environment on creep behavior of Nexte720/alumina ceramic composite at elevated temperature[J].Materials Science and Engineering: A2008497(1/2):101-110.
[15]
RUGGLES-WRENN M B KUTSAL T.Effects of steam environment on creep behavior of Nexte720/alumina-mullite ceramic composite at elevated temperature[J].Composites Part A201041(12):1807-1816.
[16]
STAEHLER J M ZAWADA L P.Performance of four ceramic-matrix composite divergent flap inserts following ground testing on an F110 turbofan engine[J].Journal of the American Ceramic Society200083(7):1727-1738.
[17]
CARELLI E A V FUJITA H YANG J Y,et al.Effects of thermal aging on the mechanical properties of a porous matrix ceramic composite[J].Journal of the American Ceramic Society200285(3):595-602.
[18]
CHAWLA K K COFFIN C XU Z R.Interface engineering in oxide fibre/oxide matrix composites[J].International Materials Reviews200045(5):165-189.
[19]
HE M Y HUTCHINSON J W.Crack deflection at an interface between dissimilar elastic materials[J].International Journal of Solids and Structures198925(9):1053-1067.
[20]
WANG Y ZHANG A LI G D,et al.Sintering temperature and interphase effects on mechanical properties of an oxide fiber-reinforced Al2O3-SiO2 composite fabricated by sol-gel method[J].Applied Composite Materials202128(2):321-339.
[21]
SHI Y HÖNIG S FRIEß M,et al.Manufacture and characterization of oxide ceramic matrix composites out of commercial pre-impregnated fabrics[J].Ceramics International201844(2):2320-2327.

基金

国家自然科学基金项目(U2241239)

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