K439B镍基高温合金不同壁厚平板件铸态组织特征

周德鹏, 隋大山, 麻晋源, 桂大兴, 董安平, 孙宝德

PDF(3621 KB)
PDF(3621 KB)
材料工程 ›› 2025, Vol. 53 ›› Issue (1) : 91-98. DOI: 10.11868/j.issn.1001-4381.2023.000808
研究论文

K439B镍基高温合金不同壁厚平板件铸态组织特征

作者信息 +

As-cast microstructure characteristics of K439B nickel-based superalloy thin- walled castings of different thickness

Author information +
History +

摘要

K439B是一种服役温度可达800 ℃以上的新型镍基高温合金,由于铸件结构向着薄壁化方向发展,有必要开展K439B合金薄壁铸件的微观组织特征研究。为此设计了壁厚分别为1 mm和2 mm的薄壁铸件,进行了精密铸造实验和数值模拟。铸件的铸态组织对比分析表明,壁厚1 mm和2 mm薄壁的枝晶生长方向均为沿型壁指向中心,区别在于1 mm薄壁的枝晶生长方向与型壁夹角更接近垂直,并且1 mm和2 mm薄壁的平均一次枝晶臂间距分别为60.64 μm和46.23 μm;平均二次枝晶臂间距分别为19.31 μm和22.69 μm;并且1 mm薄板的平均晶粒尺寸为216.61 μm,2 mm薄板的平均晶粒尺寸为239.11 μm。结合数值模拟分析表明,枝晶臂间距与温度梯度和冷却速率的关系趋势基本符合已有的经验公式,但是当壁厚减小到某临界厚度时,一次枝晶臂间距与温度梯度和冷却速率的关系不再简单符合该经验公式。实验和模拟分析结果为合理制订K439B合金薄壁件的铸造工艺提供了参考和借鉴。

Abstract

K439B is a new type of nickel-based superalloy with a service temperature up to 800 ℃. In the face of the demand for mass reduction of aircraft, the structure of its components is developing in the direction of thin-wall. Thus, it is necessary to study the microstructure of the K439B alloy thin-walled castings. For this purpose, the thin-wall castings with wall thicknesses of 1 mm and 2 mm are designed, and gravity investment casting experiments and numerical simulations are conducted. Comparative analysis of the as-cast microstructure of the castings shows that the growth directions of the dendrites in both 1 mm and 2 mm thin-wall are along the shell wall pointing to the center, the difference is that the growth directions of the dendrites in the 1 mm thin-wall are closer to the vertical angle with the wall. The average primary dendrite arm spacings (PDAS) are 60.64 μm for 1 mm thin-wall and 46.23 μm for 2 mm thin-wall, respectively. The average secondary dendrite arm spacings (SDAS) are 19.31 μm for 1 mm thin-wall and 22.69 μm for 2 mm thin-wall, separately. Meanwhile, the average grain size of the 1 mm thin-wall is 216.61 μm, and the corresponding size of the 2 mm thin-wall is 239.11 μm. Combined with numerical simulation analysis, it is shown that the relationship trend between dendrite arm spacings, temperature gradient, and cooling rate basically matches the existing empirical formula, but the relationship between PDAS and temperature gradient and cooling rate no longer simply matches the formula when the wall thickness is reduced to a certain critical thickness. These results of the experimental and simulation analysis could provide a reference to rationally design the casting process for the K439B nickel-based superalloy thin-walled casting crafts.

关键词

K439B镍基高温合金 / 薄壁铸件 / 枝晶臂间距 / 晶粒尺寸 / 数值模拟

Key words

K439B nickel-based superalloy / thin-wall casting / dendrite arm spacing / grain size / numerical simulation

中图分类号

TG146.1+5 / TB31

引用本文

导出引用
周德鹏 , 隋大山 , 麻晋源 , . K439B镍基高温合金不同壁厚平板件铸态组织特征. 材料工程. 2025, 53(1): 91-98 https://doi.org/10.11868/j.issn.1001-4381.2023.000808
Depeng ZHOU, Dashan SUI, Jinyuan MA, et al. As-cast microstructure characteristics of K439B nickel-based superalloy thin- walled castings of different thickness[J]. Journal of Materials Engineering. 2025, 53(1): 91-98 https://doi.org/10.11868/j.issn.1001-4381.2023.000808

参考文献

[1]
WU Y LI C XIA X, et al. Precipitate coarsening and its effects on the hot deformation behavior of the recently developed γ′-strengthened superalloys [J]. Journal of Materials Science & Technology202167: 95-104.
[2]
施建军,操光辉.激光选区熔化Inconel 718合金抗氧化性能研究[J].上海金属202345(6):55-62.
SHI J J CAO G H. Research on oxidation resistance of Inconel 718 alloy fabricated by selective laser melting [J]. Shanghai Metals202345(6): 55-62.
[3]
陈晶阳,任晓冬,张明军,等.铸造镍基高温合金K439B的组织及典型性能[J].金属热处理202348(1):100-104.
CHEN J Y REN X D ZHANG M J, et al. Microstructure and typical properties of cast Ni-based superalloy K439B [J]. Heat Treatment of Metals202348(1): 100-104.
[4]
张雷雷,陈晶阳,汤鑫,等.K439B铸造高温合金800 ℃长期时效组织与性能演变[J].金属学报202359(9):1253-1264.
ZHANG L L CHEN J Y TANG X, et al. Evolution of microstructures and mechanical properties of K439B equiaxed superalloy during long-term aging at 800 ℃ [J]. Acta Metallurgica Sinica202359(9): 1253-1264.
[5]
张雷雷,陈晶阳,骞磊,等.浇注温度对K439B合金显微组织和力学性能的影响[J].材料热处理学报201940(9):57-63.
ZHANG L L CHEN J Y QIAN L, et al. Effect of casting temperature on microstructure and mechanical properties of K439B superalloy [J]. Transactions of Materials and Heat Treatment201940(9): 57-63.
[6]
张雷雷,陈晶阳,任晓冬,等.固溶参数对镍基高温合金K439B显微组织及力学性能的影响[J].材料工程202452(4):120-126.
ZHANG L L CHEN J Y REN X D, et al. Effect of solution parameters on microstructures and mechanical properties of K439B nickel-based superalloy [J]. Journal of Materials Engineering202452(4):120-126.
[7]
张明军,张雷雷,胡颖涛,等.热等静压处理对K439B高温合金显微组织的影响[J].金属热处理202045(11):177-181.
ZHAGN M J ZHAGN L L HU Y T, et al. Effect of hot isostatic pressing on microstructure of K439B superalloy [J]. Heat Treatment of Metals202045(11): 177-181.
[8]
鄯宇,隋大山,麻晋源,等.K439B镍基合金精密铸造微观组织模拟与实验验证[J].稀有金属202347(7):923-933.
SHAN Y SUI D S MA J Y, et al. Numerical simulation and experimental verification of microstructure evolution for K439B nickel-based superalloy in investment casting process [J]. Chinese Journal of Rare Metals202347(7): 923-933.
[9]
LI Z ZHANG Z L WU A P, et al. Microstructure and mechanical properties of laser welded and post-weld heat-treated K439B superalloy [J]. Transactions of Nonferrous Metals Society of China202434(3):905-917.
[10]
黄新春, 史恺宁,张定华. 航空发动机智能加工技术进展研究[J]. 航空精密制造技术202258(2):1-5.
HUANG X C SHI K N ZHANG D H. Research on the progress of aero-engine intelligent manufacturing technology [J]. Aviation Precision Manufacturing Technology202258(2): 1-5.
[11]
赵罡, 李瑾岳, 徐茂程,等. 航空发动机关键装配技术综述与展望[J]. 航空学报202243(10): 527484.
ZHAO G LI J Y XU M C, et al. Research status and prospect of key aero-engine assembly technology [J]. Acta Aeronautica et Astronautica Sinica202243(10): 527484.
[12]
程亚珍, 李渤渤, 孙冰,等. 薄壁复杂钛合金铸件熔模铸造工艺模拟及优化[J]. 特种铸造及有色合金202242(6):780-784.
CHEN Y Z LI B B SUN B, et al. Numerical simulation and process optimization of investment casting process for thin-walled complex titanium alloy casting [J]. Special Casting & Nonferrous Alloys202242(6): 780-784.
[13]
何树先, 王俊.大型复杂薄壁高温合金铸件熔模精铸技术的研究进展[J].热加工工艺201342(21): 5-12.
HE S X WANG J. Development on investment casting of large thin wall complex superalloy castings [J]. Hot Working Technology201342(21): 5-12.
[14]
NAWROCKI J MOTYKA M SZELIGA D, et al. Effect of cooling rate on macro- and microstructure of thin-walled nickel superalloy precision castings [J]. Journal of Manufacturing Processes202049: 153-161.
[15]
KOERBER S FLECK M VOELKL R, et al. Anisotropic growth of the primary dendrite arms in a single-crystal thin-walled nickel-based superalloy [J]. Advanced Engineering Materials202224(6): 2101332.
[16]
GORNY M KAWALEC M WITEK G, et al. The influence of wall thickness and mould temperature on structure and properties of thin wall ductile iron castings [J]. Archives of Foundry Engineering201919(2): 55-59.
[17]
李剑锋,周铁涛,燕平,等.一种镍基单晶高温合金凝固组织的截面尺寸效应[J]. 材料工程2009(6):20-25.
LI J F ZHOU T T YAN P, et al. Effects of section sizes on microstructure of a nickel-base single crystal superalloy [J]. Journal of Materials Engineering2009(6): 20-25.
[18]
孙智, 吴国清, 纪志军,等. 薄壁ZTC4钛合金铸件表层与心部组织性能分析[J]. 铸造工程202246(4):1-6.
SUN Z WU G Q JI Z J, et al. Analysis of surface and central microstructure and properties of a thin-walled ZTC4 titanium alloy casting [J]. Foundry Engineering202246(4): 1-6.
[19]
HUNT J D. Solidification and casting of metals [M]. London: The Metals Society, 1979.
[20]
WILLS V A MCCARTNEY D G. A comparative study of solidification features in nickel-base superalloys: microstructural evolution and microsegregation [J]. Materials Science and Engineering: A1991145(2): 223-232.
[21]
YANG L LI J R. Effect of section size on the microstructure of thin-walled specimen of DD6 single crystal superalloy [J]. Rare Metal Materials and Engineering201544(6): 1363-1368.

基金

国家科技重大专项(J2019-Ⅵ-0004-0117)
上海市产业协同创新项目(XTCX-KJ-2022-41)

评论

PDF(3621 KB)

Accesses

Citation

Detail

段落导航
相关文章

/