冷拉07Cr17Ni7Al微细丝材的组织及性能演变规律

何钦生, 王建桥, 赵振, 李方, 张十庆, 王宏, 邹兴政, 唐远寿, 黄敏, 黎静

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材料工程 ›› 2025, Vol. 53 ›› Issue (3) : 83-94. DOI: 10.11868/j.issn.1001-4381.2023.000785
研究论文

冷拉07Cr17Ni7Al微细丝材的组织及性能演变规律

作者信息 +

Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire

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摘要

材料的弹性极限是弹簧设计中极为重要的参数,对弹簧的特性有显著影响。针对直径为0.3 mm的阀门弹簧用07Cr17Ni7Al微细丝,通过室温拉伸、单臂弯曲法、光学显微镜、X射线衍射、扫描电镜研究了冷拉拔变形量对丝材强度、弹性极限、弹性后效和微观组织的影响,采用不同数学模型对变形量-马氏体含量、变形量-弹性极限、应力-弹性后效进行了分析。结果表明:固溶态07Cr17Ni7Al丝材由奥氏体和少量铁素体组成,冷拉拔使奥氏体转变为马氏体,随变形量增大,形变诱发马氏体增加。马氏体含量-冷拉等效应变关系符合Olson-Cohen模型,当冷拉等效应变达到1.64时,马氏体含量约92%,形变诱发马氏体达到饱和。丝材的抗拉强度-冷拉等效应变呈线性关系,变形量越大,抗拉强度越高。弹性极限随变形量增大而提高,弹性极限-冷拉等效应变呈“S”形曲线关系,且符合DoseResp模型,当冷拉等效应变达到1.64以上,弹性极限提高程度变小并趋于平缓。弹性后效随应力的提高而增加,符合PWL2模型,存在“弹性后效临界应力”,当应力超过该临界值后,弹性后效随应力增加的速率会提高2~11倍。冷拉等效应变为1.64~2.41时,丝材具有良好的力学性能和弹性性能。

Abstract

The elastic limit is a critical parameter in spring design, which has a significant impact on the spring characteristic. The influence of cold drawing on the strength, elastic limit, elastic after-effect, and microstructure of 07Cr17Ni7Al ultrafine wire with a diameter of 0.3 mm for valve springs is investigated using room temperature tensile tests, single arm bending method, optical microscope(OM), X-ray diffraction(XRD) and scanning electron microscope(SEM). Different mathematical models are used to fit and analyze the deformation and martensite content, deformation-elastic limit, and stress-elastic after-effect. The results show that the solid solution 07Cr17Ni7Al wire is composed of austenite and a small amount of ferrite. Cold drawing transforms austenite into martensite, the content of deformation-induced martensite (DIM) increases with increasing deformation. The relationship between DIM content and cold-drawn equivalent strain (η) conforms to the Olson-Cohen model. When η reaches 1.64, the DIM content is about 92%, and the DIM reaches saturation. The tensile strength of wire exhibits a linear relationship with η, and the larger the deformation, the higher the tensile strength. The relationship between the elastic limit and the η follows an “S” shaped curve and conforms to the DoseResp model. The elastic limit increases with increasing deformation. When the η reaches 1.64 or more, the elastic limit tends to be gentle. The elastic after-effect increases with increasing stress, which conforms to the PWL2 model. There exists a “critical stress for elastic after-effect”. When the stress exceeds this critical value, the rate of elastic after-effect increases by 2-11 times with increasing stress. When the η is 1.64-2.41, the 07Cr17Ni7Al wire has good mechanical and elastic properties.

关键词

不锈钢 / 形变诱发马氏体 / 弹性极限 / 弹性后效 / 力学性能 / 微细丝 / 冷拉拔

Key words

stainless steel / deformation-induced martensite / elastic limit / elastic after-effect / mechanical property / ultrafine wire / cold drawing

中图分类号

TB31 / TG142.1 / TG356.4

引用本文

导出引用
何钦生 , 王建桥 , 赵振 , . 冷拉07Cr17Ni7Al微细丝材的组织及性能演变规律. 材料工程. 2025, 53(3): 83-94 https://doi.org/10.11868/j.issn.1001-4381.2023.000785
Qinsheng HE, Jianqiao WANG, Zhen ZHAO, et al. Evolution of microstructure and properties of cold-drawn 07Cr17Ni7Al ultrafine wire[J]. Journal of Materials Engineering. 2025, 53(3): 83-94 https://doi.org/10.11868/j.issn.1001-4381.2023.000785

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基金

国机研究院青年科研基金项目(SINOMAST-QNJJ-2022-03)
重庆英才·创新创业示范团队项目(CQYC202003182)
重庆英才·创新领军人才项目(cstc2022ycjh-bgzxm0217)

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