微波养护对水泥砂浆性能与微观结构的影响

刘伊迪, 孙明刚, 王立峰, 李双欣, 李旭森, 凌民海, 杨英姿

PDF(5715 KB)
PDF(5715 KB)
森林工程 ›› 2025, Vol. 41 ›› Issue (03) : 614-628. DOI: 10.7525/j.issn.1006-8023.2025.03.018
道路与交通

微波养护对水泥砂浆性能与微观结构的影响

作者信息 +

Effect of Microwave Curing on Properties and Microstructure of Cement Mortar

Author information +
History +

摘要

混凝土微波养护技术可以显著提高混凝土早期强度,但微波养护制度没有统一的设计标准,导致养护后材料性能呈现较大差异。为探究微波养护制度的影响,采用响应面法系统分析微波养护参数对水泥砂浆抗压强度的影响规律。建立关键微波养护参数与材料性能之间的关系模型,确定加热温度控制在40 ℃以下、加热功率为1 000 W、加热时间为 30 min为最佳微波养护制度。通过运用X射线衍射(XRD)、压汞法(MIP)以及扫描电子显微镜(SEM)等测试方法,分析微波养护对水泥材料化学成分及微观结构的影响,揭示合理的微波养护制度能够促进砂浆的水化程度并形成更加致密的结构。通过计算机模拟对微波养护过程中的温度变化进行分析,发现微波养护温度具有热点效应。进一步得出微波养护温度是影响砂浆强度最关键的影响因素。

Abstract

Microwave curing technology of concrete can significantly improve the early strength of concrete, but there is no uniform design standard for microwave curing method, resulting in great differences in material properties after curing. To explore the influence of microwave curing methods, this study employed the response surface methodology to systematically analyze the influence of microwave curing method on the compressive strength of cement mortar. The relationship model between key microwave curing parameters and material properties was established, and the optimal microwave curing method was determined when the heating temperature was under 40℃ and the heating power was 1 000 W for 30 min. Chemical components and microstructure impacts were studied using X-ray diffraction (XRD), mercury intrusion porosimetry (MIP), and scanning electron microscope (SEM), and it was revealed that a reasonable microwave curing method can promote the hydration degree of mortar and form a denser structure. The temperature variation in microwave curing process was analyzed by combining experimental data and computer simulation, and it was found that microwave curing temperature had hot spot effect. It is concluded that microwave curing temperature is the most important factor affecting the strength of mortar.

关键词

响应面法 / 微波养护 / 砂浆 / 抗压强度 / 微观结构

Key words

Response surface methodology / microwave curing / mortar / compressive strength / microstructure

中图分类号

TU528

引用本文

导出引用
刘伊迪 , 孙明刚 , 王立峰 , . 微波养护对水泥砂浆性能与微观结构的影响. 森林工程. 2025, 41(03): 614-628 https://doi.org/10.7525/j.issn.1006-8023.2025.03.018
LIU Yidi, SUN Minggang, WANG Lifeng, et al. Effect of Microwave Curing on Properties and Microstructure of Cement Mortar[J]. Forest Engineering. 2025, 41(03): 614-628 https://doi.org/10.7525/j.issn.1006-8023.2025.03.018

参考文献

1
Open energy data initiative (OEDI)[EB/OL].[2024-05-24].
2
Emissions gap report 2023:Broken record-Temperatures hit new highs, yet world fails to cut emissions (again)[EB/OL].[2024-05-24].
3
HAN Y PARK K B YANG B,et al.Optimizing and designing the effects of microwave pre-curing on the properties of ternary blended concrete with slag and fly ash using the simplex centroid method[J].Construction and Building Materials2024419:135443.
4
ASOMANING J HAUPT S CHAE M,et al.Recent developments in microwave-assisted thermal conversion of biomass for fuels and chemicals[J].Renewable and Sustainable Energy Reviews201892:642-657.
5
高小建,李双欣.微波养护对掺矿渣超高性能混凝土力学性能的影响及机理[J].材料导报201933(2):271-276.
GAO X J LI S X.Effects of microwave curing on the mechanical properties of ultra-high performance concrete and affecting mechanism[J].Materials Reports201933(2):271-276.
6
ZHOU F PAN G MENG H,et al.Effect of secondary curing on the performance of microwave cured concrete[J].Construction and Building Materials2022330:127256.
7
BUTTRESS A JONES A KINGMAN S.Microwave processing of cement and concrete materials – towards an industrial reality?[J].Cement and Concrete Research201568:112-123.
8
WU X Q DONG J B TANG M S.Microwave curing technique in concrete manufacture[J].Cement and Concrete Research198717(2):205-210.
9
牛旭婧,许雍久,朱可欣,等.微波养护对活性粉末混凝土力学性能的影响[J].华中科技大学学报(自然科学版):1-8.
NIU X J XU Y J ZHU K X,et al.Effects of microwave curing on mechanical properties of reactive powder concrete[J].Journal of Huazhong University of Science and Technology(Natural Science Edition):1-8.
10
GAO Z HE Y LI M,et al.Impacts of microwave on hydration evolution of Portland cement in the perspective of composition and microstructure of hydrates[J].Construction and Building Materials2022360:129569.
11
WANG S CHEN F YU M,et al.Exploring the effect of the micropore on the microstructure development of low water-cement ratio composite (LW/B-CC) subjected to microwave pre-curing[J].Construction and Building Materials2024416:135141.
12
KONG Y WANG P LIU S,et al.Hydration and microstructure of cement-based materials under microwave curing[J].Construction and Building Materials2016114:831-838.
13
MAKUL N RATTANADECHO P AGRAWAL D K.Applications of microwave energy in cement and concrete – A review[J].Renewable and Sustainable Energy Reviews201437:715-733.
14
LEUNG C K Y PHEERAPHAN T.Determination of optimal process for microwave curing of concrete[J].Cement and Concrete Research199727(3):463-472.
15
MANGAT P S GRIGORIADIS K ABUBAKRI S.Microwave curing parameters of in-situ concrete repairs[J].Construction and Building Materials2016112:856-866.
16
SHEN J LI Y LIN H,et al.The experimental study on microwave-assisted preparation of Ultra-High Performance Geopolymer Concrete (UHPGC)[J].Construction and Building Materials2024414:134934.
17
王红,董双快,郭爽,等.基于响应面法的水泥-粉煤灰-矿粉浆体流变分析[J].建筑结构202252(S1):1576-1581.
WANG H DONG S K GUO S,et al.Rheological analysis of cement-fly ash-ore slurry based on response surface method[J].Building Structure202252(S1):1576-1581.
18
胡豪,吴鹤翔,孙全胜.基于响应面法的悬拼优化施工中混合梁斜拉桥响应分析[J].森林工程202238(6):115-123.
HU H WU H X SUN Q S.Response analysis of hybrid girder cable-stayed bridge in cantilever assembly optimization based on the response surface method[J].Forest Engineering202238(6):115-123.
19
刘子仪,宋少民.基于响应面法的混杂纤维-复合胶凝材料体系优化设计[J].硅酸盐通报202342(12):4197-4207,4215.
LIU Z Y SONG S M.Optimal design of hybrid fiber-composite cementitious material system based on response surface methodolog[J].Bulletin of the Chinese Ceramic Society202342(12):4197-4207,4215.
20
TIONG K Y MA Z PALMQVIST C W.Analyzing factors contributing to real-time train arrival delays using seemingly unrelated regression models[J].Transportation Research Part A:Policy and Practice2023174:103751.
21
WAGHE U AGRAWAL D ANSARI K,et al.Enhancing eco-concrete performance through synergistic integration of sugarcane,metakaolin,and crumb rubber:Experimental investigation and response surface optimization[J].Journal of Engineering Research202312(4):645-658.
22
PENG Q CHEN B LU Q,et al.Effect of steel-waste PET hybrid fiber on properties of recycled aggregate concrete based on response surface methodology[J].Construction and Building Materials2023397:132448.
23
FENG X LIU Q WANG C.A lack-of-fit test for quantile regression process models[J].Statistics & Probability Letters2023192:109680.
24
JAVIER K R A CAMACHO D H.Dataset on the optimization by response surface methodology for the synthesis of silver nanoparticles using Laxitextum bicolor mushroom[J].Data in Brief202245:108631.
25
ABDELLATIEF M ELRAHMAN M A ELGENDY G,et al.Response surface methodology-based modelling and optimization of sustainable UHPC containing ultrafine fly ash and metakaolin[J].Construction and Building Materials2023388:131696.
26
温红宁,金俊松,章一丁,等.基于响应面法的FGH4113A高温合金涡轮盘锻造工艺参数优化[J].稀有金属材料与工程202453(9):2633-2641.
WEN H N JIN J S ZHANG Y D,et al.Optimization of forging processing parameters of the FGH4113A P/M superalloy turbine disk based on response surface method[J].Rare Metal Materials and Engineering202453(9):2633-2641.
27
ZHANG J YU R SHUI Z,et al.Hydration kinetics and microstructure development of Ultra-High Performance Concrete (UHPC) subjected to microwave pre-curing[J].Cement and Concrete Composites2022129:104484.
28
张照鹏,褚忠信,李应坤.峰高与峰面积统计量表示岩心黏土矿物相对含量的差异[J].海洋科学201640(12):107-113.
ZHANG Z P CHU Z X LI Y K.Difference between peak-height and peak-area methods in extracting relative contents of core clay minerals[J].Marine Sciences201640(12):107-113.
29
赵国庆,杨进波,尹航.C-S-H凝胶无定型纳米孔隙中NaCl蒸发结晶分子动力学分析[J].硅酸盐通报202443(9):3173-3181.
ZHAO G Q YANG J B YIN H.Molecular dynamics of NaCl evaporation crystallization in C-S-H gel amorphous nanopores[J].Bulletin of the Chinese Ceramic Society202443(9):3173-3181.
30
SUN D WANG X WANG J,et al.Properties and hydration characteristics of cementitious blends with two kinds of solid waste-based sulfoaluminate cement[J].Construction and Building Materials2024411:134482.
31
ZHANG X HAYWARD D O MINGOS D M P.Effects of microwave dielectric heating on heterogeneous catalysis[J].Catalysis Letters200388(1):33-38.
32
XU G TIAN Q MIAO J,et al.Early-age hydration and mechanical properties of high volume slag and fly ash concrete at different curing temperatures[J].Construction and Building Materials2017149:367-377.
33
VU V H TRAN B V LE B A,et al.Prediction of the relationship between strength and porosity of pervious concrete:A micromechanical investigation[J].Mechanics Research Communications2021118:103791.
34
AHMAD M R CHEN B YU J.A comprehensive study of basalt fiber reinforced magnesium phosphate cement incorporating ultrafine fly ash[J].Composites Part B:Engineering2019168:204-217.
35
RATTANADECHO P MAKUL N PICHAICHERD A,et al.A novel rapid microwave-thermal process for accelerated curing of concrete:Prototype design,optimal process and experimental investigations[J].Construction and Building Materials2016123:768-784.
36
PATEL H H BLAND C H POOLE A B.The microstructure of concrete cured at elevated temperatures[J].Cement and Concrete Research199525(3):485-490.
37
孙嘉伦,张春晓,毛继泽,等.养护制度对超高性能混凝土强度的影响机理[J].材料导报202438(18):66-70.
SUN J L ZHANG C X MAO J Z,et al.Affecting mechanism of curing regimes on the strength of ultra-high performance concrete[J].Materials Reports202438(18):66-70.

基金

国家自然科学基金青年科学基金项目(52108193)
黑龙江省重点研发计划(JD22A012)
龙建路桥股份有限公司科技项目(230000100004258230003)

评论

PDF(5715 KB)

Accesses

Citation

Detail

段落导航
相关文章

/